化工社化工社 化学情報印刷レポート · 研究参考用
2,3-Dichloro-1,3-butadiene → Formaldehyde
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 2,3-Dichloro-1,3-butadiene | HCID 15447 | — |
| 反応物 | Resorcinol-formaldehyde resin | HCID 159980 | — |
| 反応物 | Sodium Lauryl Sulfate | HCID 3423265 | — |
| 溶媒 | Water | HCID 962 | — |
| 生成物 | Formaldehyde | HCID 712 | — |
| 生成物 | Resorcinol | HCID 5054 | — |
| 生成物 | Resorcinol-formaldehyde resin | HCID 159980 | — |
反応手順
18.0 g of sodium lauryl sulfate (Emar 2F Needle (30% concentration), manufactured by Kao Corporation) was added as a surfactant to 295 g of the above 2,3-dichlorobutadiene homopolymer latex (2), and the mixture was thoroughly stirred until it became uniform. Then, 264.4 g of water was added thereto, and 656.4 g of the resorcinol/formaldehyde mixed liquid prepared as described above, was mixed thereto. The mixture was left to stand and aged at 23° C. for 24 hours to obtain a resorcinol/formaldehyde/latex mixed liquid (the weight ratio of the latex solid content to the sum of resorcinol and formaldehyde: 1/0.86, total amount of surfactant: 0.74 wt %).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05766762 |
| 出典データセット | uspto-grants-1998_06 |
| ORD ID | ord-dfa1ef8ca5db49809baafea8708a917a |
| 出典メモ | uspto-grants-1998_06 |