化工社化工社 化学情報印刷レポート · 研究参考用
2-Methylpyridine 1-oxide → 2-[2-(4-Methoxy-phenyl)-vinyl]-pyridine 1-oxide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 2-Methylpyridine 1-oxide | HCID 13602 | — |
| 反応物 | 4-Methoxybenzaldehyde | HCID 31244 | — |
| 反応物 | Potassium tert-butoxide | HCID 23665647 | — |
| 生成物 | 2-[2-(4-Methoxy-phenyl)-vinyl]-pyridine 1-oxide | HCID 69592112 | — |
反応手順
Following the general method described in example 2a, 2-picoline-1-oxide was reacted with potassium tert.-butanolate and p-anisaldehyde. After extraction and chromatography the title compound was obtained as a yellow solid material. MS: m/e=227 (M+).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06951875B2 |
| 出典データセット | uspto-grants-2005_10 |
| ORD ID | ord-d36fc8c92df14c929ae703075c83232c |
| 出典メモ | uspto-grants-2005_10 |