関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Water | HCID 962 | — |
| 反応物 | Sulfuric Acid | HCID 1118 | — |
| 反応物 | 2,4,6-Trimethylphenylacetonitrile | HCID 520698 | — |
| 生成物 | Mesitylacetic acid | HCID 78123 | — |
反応手順
155 g (2,4,6-trimethylphenyl)acetonitrile are added to a solution of 1.1 L of water and 915 mL of concentrated sulfuric acid heated to 50° C. The mixture is refluxed for 6 hours with stirring. Then the reaction mixture is poured onto 3 kg of ice. The solid is suction filtered and washed with water. Yield: 131 g (86%); melting point: 163° C.-166° C.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US06951888B2 |
|---|
| 出典データセット | uspto-grants-2005_10 |
|---|
| ORD ID | ord-61a96cad4476460eaf917227b47a8666 |
|---|
| 出典メモ | uspto-grants-2005_10 |
|---|
