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HRID 967352作成日:2026年10月26日

Hexanamide, 2-hydroxy- → 5-Butyloxazolidine-2,4-dione

https://huagongshe.com/reaction/967352

反応式

関与物質

役割名称HCID仕込み量
反応物Hexanamide, 2-hydroxy-HCID 9833961—
反応物5-Butyl-oxazolidin-2,4-dione sodium saltHCID 69745152—
生成物5-Butyloxazolidine-2,4-dioneHCID 9942204—

反応手順

A part of the reaction solution was sampled and the components of the reaction solution were analyzed by HPLC, as a result, the concentration of the starting material 2-hydroxyhexanoic acid amide was 1.3 mass % in the solution and the concentration of 5-butyl-oxazolidin-2,4-dione sodium salt as the objective product was 25.9 mass % in the solution. From these analysis values, the conversion of 2-hydroxyhexanoic acid amide was 93.8% and the yield in terms of 5-butyl-oxazolidin-2,4-dione was 88.7%.

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US06953859B2
出典データセットuspto-grants-2005_10
ORD IDord-982b82a241964626b2262cc05b40d0c2
出典メモuspto-grants-2005_10