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Hexanamide, 2-hydroxy- → 5-Butyloxazolidine-2,4-dione
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Hexanamide, 2-hydroxy- | HCID 9833961 | — |
| 反応物 | 5-Butyl-oxazolidin-2,4-dione sodium salt | HCID 69745152 | — |
| 生成物 | 5-Butyloxazolidine-2,4-dione | HCID 9942204 | — |
反応手順
A part of the reaction solution was sampled and the components of the reaction solution were analyzed by HPLC, as a result, the concentration of the starting material 2-hydroxyhexanoic acid amide was 1.3 mass % in the solution and the concentration of 5-butyl-oxazolidin-2,4-dione sodium salt as the objective product was 25.9 mass % in the solution. From these analysis values, the conversion of 2-hydroxyhexanoic acid amide was 93.8% and the yield in terms of 5-butyl-oxazolidin-2,4-dione was 88.7%.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06953859B2 |
| 出典データセット | uspto-grants-2005_10 |
| ORD ID | ord-982b82a241964626b2262cc05b40d0c2 |
| 出典メモ | uspto-grants-2005_10 |