関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | 2-Bromoanisole | HCID 11358 | — |
| 反応物 | EP-302 | HCID 62790 | — |
| 反応物 | Tris(4-hydroxyphenyl)phosphine oxide | HCID 4183961 | — |
| 反応物 | HCID 178527022 | HCID 178527022 | — |
| 生成物 | Tris(4-hydroxyphenyl)phosphine Oxide EPON 828 | HCID 131725192 | — |
反応手順
A mixture of tris(4-hydroxyphenyl)phosphine oxide (prepared in a method analogous to example 2a,b using three equivalents of bromoanisole) (21.2 g) with EPON 828 (79.3 g) was heated over a 7 min period to 150° C. The mixture to this point was a slurry of the phosphine oxide in EPON 828. In the next 4 min., the pot reached a temperature of 180° C., and this point a portion of the phosphine oxide aggregated into a polymeric mass.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US06955851B2 |
|---|
| 出典データセット | uspto-grants-2005_10 |
|---|
| ORD ID | ord-83760bac48034df7ab3109825569caee |
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| 出典メモ | uspto-grants-2005_10 |
|---|
