3-Pentanol → 4-(1-Ethyl-propoxy)-2,5-dimethyl-6-(2,4,6-trimethylbenzyl)-pyrimidine

反応式

Cl[C:2]1[C:7]([CH3:8])=[C:6]([CH2:9][C:10]2[C:15]([CH3:16])=[CH:14][C:13]([CH3:17])=[CH:12][C:11]=2[CH3:18])[N:5]=[C:4]([CH3:19])[N:3]=1.[CH3:20][CH2:21][CH:22]([OH:25])[CH2:23][CH3:24]>>[CH2:21]([CH:22]([O:25][C:2]1[C:7]([CH3:8])=[C:6]([CH2:9][C:10]2[C:15]([CH3:16])=[CH:14][C:13]([CH3:17])=[CH:12][C:11]=2[CH3:18])[N:5]=[C:4]([CH3:19])[N:3]=1)[CH2:23][CH3:24])[CH3:20]

参加物

反応物 2

HCID 114283-Pentanol

HCID 219124244-Chloro-2,5-dimethyl-6-(2,4,6-trimethyl-benzyl)pyrimidine

生成物 1

HCID 98535424-(1-Ethyl-propoxy)-2,5-dimethyl-6-(2,4,6-trimethylbenzyl)-pyrimidine

実験手順

The title compound was prepared by the method analogous to that in Example 32 starting with 4-Chloro-2,5-dimethyl-6-(2,4,6-trimethyl-benzyl)-pyrimidine and 3-pentanol. White crystals. mp. 82-84° C.

出典と根拠

ORDレコード: ord-6efb34be90064848a2286026e327c157
出典データセット: uspto-grants-2005_10
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US06956047B1

反応ノート

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