3,4-Difluorobenzylamine → HCID 20729568、化合物
反応式
ClC(Cl)(Cl)[C:3]([C:5]1[NH:9][CH:8]=[C:7]([C:10](=[O:13])[CH2:11][CH3:12])[CH:6]=1)=[O:4].[F:16][C:17]1[CH:18]=[C:19]([CH:22]=[CH:23][C:24]=1[F:25])[CH2:20][NH2:21]>CN(C=O)C>[F:16][C:17]1[CH:18]=[C:19]([CH:22]=[CH:23][C:24]=1[F:25])[CH2:20][NH:21][C:3]([C:5]1[NH:9][CH:8]=[C:7]([C:10](=[O:13])[CH2:11][CH3:12])[CH:6]=1)=[O:4]参加物
4
実験手順
To a solution of compound 2 (1 equivalent) in DMF, at ambient temperature, was added 3,4-difluorobenzyl amine (1.2 equivalents). After 24 hours, the solvent was evaporated and the crude product 5 was used without purification.
後処理
- customthe solvent was evaporated
- customthe crude product 5 was used without purification
出典と根拠
- ORDレコード
- ord-380041cdd0114a85aaed2f07d1dd3798
- 出典データセット
- uspto-grants-2007_12
- 特許番号
- US07304061B2
反応ノート
読み込み中…