化工社化工社 化学情報印刷レポート · 研究参考用
2-Methylimidazole → 2-(2-Methyl-1H-imidazol-1-yl)ethan-1-amine
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 2-Methylimidazole | HCID 12749 | — |
| 反応物 | 2-Chloroethylamine hydrochloride | HCID 9793737 | — |
| 生成物 | 2-(2-Methyl-1H-imidazol-1-yl)ethan-1-amine | HCID 3157480 | 47% |
反応手順
2-(2-Methylimidazol-1-yl)ethylamine was prepared from 2-methylimidazole and 2-chloroethylamine hydrochloride using the method described in Step B of Example 1. This material was obtained as a light yellow oil in 47% yield. 1H NMR (300 MHz, CD3OD) δ 6.95 (br s, 1H), 6.82 (br s, 1H), 4.90 (bs, 2H), 3.90 (t, J=6.9 Hz, 2H), 2.93 (t, J=6.9 Hz, 2H), 2.35 (s, 3H); MS (APCI) m/z 126 [M+H]+.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07307094B2 |
| 出典データセット | uspto-grants-2007_12 |
| ORD ID | ord-6b9488b66cbe4438850a1055f7b1eecf |
| 出典メモ | uspto-grants-2007_12 |