6-Ethylnicotinonitrile → 3-Pyridinecarbonitrile, 2-ethyl-6-methyl-

反応式

[CH3:1][C:2]1[CH:9]=[CH:8][C:5]([C:6]#[N:7])=[C:4]([CH:10]=[CH2:11])[N:3]=1.C(C1C=CC(C#N)=CN=1)C>>[CH2:10]([C:4]1[N:3]=[C:2]([CH3:1])[CH:9]=[CH:8][C:5]=1[C:6]#[N:7])[CH3:11]

参加物

反応物 2

HCID 181776766-Ethylnicotinonitrile

HCID 18362992HCID 18362992、化合物

生成物 1

HCID 183629623-Pyridinecarbonitrile, 2-ethyl-6-methyl-

実験手順

Compound 386B was prepared from 386A by a route analogous to that used for the preparation of 384B. HPLC retention time=1.18 min. (Condition A), M+=147.

出典と根拠

ORDレコード: ord-6ea5a59e541946329d8a9fb9b90b2f82
出典データセット: uspto-grants-2007_12
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US07312209B2

反応ノート

読み込み中…