化工社化工社 化学情報印刷レポート · 研究参考用
Hydroxylamine → 5-Diethylphosphono-2-furaldehyde oxime
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Hydroxylamine | HCID 787 | — |
| 反応物 | Sodium Acetate | HCID 517045 | — |
| 反応物 | Diethyl (5-formylfuran-2-yl)phosphonate | HCID 46784019 | — |
| 溶媒 | Ethanol | HCID 702 | — |
| 生成物 | 5-Diethylphosphono-2-furaldehyde oxime | HCID 86586426 | — |
反応手順
A solution of 5-diethylphosphono-2-furaldehyde (1 mmole) in ethanol was treated with hydroxylamine (1.1 mmole) and sodium acetate (2.2 mmole) at 25° C. for 12 h. Extraction and chromatography gave 5-diethylphosphono-2-furaldehyde oxime.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07312219B2 |
| 出典データセット | uspto-grants-2007_12 |
| ORD ID | ord-147f8bc2e0254f939c960b6c8d0837a5 |
| 出典メモ | uspto-grants-2007_12 |