Benzoyl chloride → HCID 21313681、化合物
反応式
[CH3:1][C:2]1[CH:3]=[C:4]([CH2:7][C:8]([OH:10])=[O:9])[S:5][CH:6]=1.[C:11](Cl)(=[O:18])[C:12]1[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=1>>[CH3:1][C:2]1[CH:3]=[C:4]([CH2:7][C:8]([OH:10])=[O:9])[S:5][C:6]=1[C:11](=[O:18])[C:12]1[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=1参加物
3
実験手順
Using the procedure of Example 15, 6.65 gm of 4-methyl-thiophene-2-acetic acid and 5.96 gm of benzoyl chloride were reacted to obtain 4.87 gm of 4-methyl-5-benzoyl-thiophene-2-acetic acid melting at 86° C. The product occurred as a colorless solid soluble in benzene, ether, ethanol, chloroform and acetone and insoluble in water.
後処理
- customwere reacted
出典と根拠
- ORDレコード
- ord-af29774f57e04e40b5d243a3431f6715
- 出典データセット
- uspto-grants-1979_07
- 特許番号
- US04159986
反応ノート
読み込み中…