Cyclohexyl isocyanate → HCID 178485086、化合物
反応式
[CH3:1][N:2]([CH3:7])[C:3]([NH2:6])=[N:4][CH3:5].[CH:8]1([N:14]=[C:15]=[O:16])[CH2:13][CH2:12][CH2:11][CH2:10][CH2:9]1>C1(C)C=CC=CC=1>[CH:8]1([NH:14][C:15]([N:6]=[C:3]([NH:4][CH3:5])[N:2]([CH3:7])[CH3:1])=[O:16])[CH2:13][CH2:12][CH2:11][CH2:10][CH2:9]1参加物
4
実験手順
To 60.6 parts by weight of 1,1,2-trimethylguanidine in 600 parts by volume of toluene are added dropwise with cooling 75 parts by weight of cyclohexyl isocyanate. After evaporation of the solvent in vacuo, the product is recrystallized from acetonitrile to yield 2-cyclohexylcarbamoyl-1,1,3-trimethylguanidine, m.p. 121°-124° C.
後処理
- customAfter evaporation of the solvent in vacuo
- customthe product is recrystallized from acetonitrile
出典と根拠
- ORDレコード
- ord-bd00a2121e2842f294c6457713ad36d7
- 出典データセット
- uspto-grants-1977_10
- 特許番号
- US04053299
反応ノート
読み込み中…