化工社化工社 化学情報印刷レポート · 研究参考用
Acetic Acid → Molybdate (Mo2O72-), hydrogen, compd. with 1,3,5-triazine-2,4,6-triamine (1:2:1)
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Acetic Acid | HCID 176 | — |
| 反応物 | Melamine | HCID 7955 | — |
| 触媒 | Azanium bis(dioxido(dioxo)molybdenum) | HCID 21895884 | — |
| 溶媒 | Water | HCID 962 | — |
| 生成物 | Molybdate (Mo2O72-), hydrogen, compd. with 1,3,5-triazine-2,4,6-triamine (1:2:1) | HCID 103335 | — |
反応手順
Melamine molybdate was prepared in the presence of acetic acid as follows. 10 grams of melamine, 9.52 grams of acetic acid, and 250 ml water were dissolved together by refluxing in a 500 ml roundbottomed flask equipped with a stirrer and water-cooled condenser. 26.95 grams of ammonium dimolybdate was dissolved in 50 ml. hot water and then added to the first solution. A white precipitate formed immediately.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04053451 |
| 出典データセット | uspto-grants-1977_10 |
| ORD ID | ord-825f184ddfa746be93a237a378810b3e |
| 出典メモ | uspto-grants-1977_10 |