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Ethylenediamine → N-(2-Dimethylaminoethyl)-N'-[2-(2-benzimidazolylmethylamino)-ethyl]thiourea
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Ethylenediamine | HCID 3301 | — |
| 反応物 | 2-Chloromethylbenzimidazole | HCID 78571 | — |
| 反応物 | (2-Isothiocyanatoethyl)dimethylamine | HCID 3853726 | — |
| 反応物 | N1-((1H-Benzo[d]imidazol-2-yl)methyl)ethane-1,2-diamine | HCID 15365342 | — |
| 生成物 | N-(2-Dimethylaminoethyl)-N'-[2-(2-benzimidazolylmethylamino)-ethyl]thiourea | HCID 54373380 | — |
反応手順
N-(2-Benzimidazolylmethyl)ethylenediamine, prepared by reacting ethylenediamine with 2-chloromethylbenzimidazole by the procedure of Example 40, is reacted with 2-dimethylaminoethyl isothiocyanate by the procedure of Example 40 to give the title compound.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04053473 |
| 出典データセット | uspto-grants-1977_10 |
| ORD ID | ord-031abe02c47d4f7cb79370ecad34900a |
| 出典メモ | uspto-grants-1977_10 |