Methyl Acrylate → HCID 53766522、化合物
反応式
[NH2:1][CH2:2][C:3]1[CH:4]=[N:5][CH:6]=[CH:7][CH:8]=1.[C:9]([O:13][CH3:14])(=[O:12])[CH:10]=[CH2:11]>>[CH3:14][O:13][C:9]([CH2:10][CH2:11][N:1]([CH2:2][C:3]1[CH:4]=[N:5][CH:6]=[CH:7][CH:8]=1)[CH2:11][CH2:10][C:9]([O:13][CH3:14])=[O:12])=[O:12]参加物
3
実験手順
52.06 Grams of 3-aminomethylpyridine was refluxed with 200 milliliters of methyl acrylate for 96 hours. The excess methyl acrylate was evaporated off to give 137.6 grams of 3-[N,N-di(2-methoxycarbonylethyl)aminomethyl] pyridine.
後処理
- customThe excess methyl acrylate was evaporated off
出典と根拠
- ORDレコード
- ord-da7af07fcf8d44359b3ca5c50a1207c6
- 出典データセット
- uspto-grants-1977_10
- 特許番号
- US04053615
反応ノート
読み込み中…