HCID 21401682、化合物 → 8-Carbamoyl-12-hydroxy-12-methylheptadecanoic acid

反応式

C(C(CCCC(OC(=O)C)CCCCC)CCCCCCC(OCC)=O)(=O)N.[C:29]([CH:32]([CH2:44][CH2:45][CH2:46][C:47]([OH:54])([CH3:53])[CH2:48][CH2:49][CH2:50][CH2:51][CH3:52])[CH2:33][CH2:34][CH2:35][CH2:36][CH2:37][CH2:38][C:39]([O:41]CC)=[O:40])(=[O:31])[NH2:30]>>[C:29]([CH:32]([CH2:44][CH2:45][CH2:46][C:47]([OH:54])([CH3:53])[CH2:48][CH2:49][CH2:50][CH2:51][CH3:52])[CH2:33][CH2:34][CH2:35][CH2:36][CH2:37][CH2:38][C:39]([OH:41])=[O:40])(=[O:31])[NH2:30]

参加物

反応物 2

HCID 21401682HCID 21401682、化合物

HCID 21401727Ethyl 8-carbamoyl-12-hydroxy-12-methylheptadecanoate

生成物 1

HCID 214016968-Carbamoyl-12-hydroxy-12-methylheptadecanoic acid

実験手順

The synthesis of this compound is carried out as described in Example 1, Step F, except that the ethyl 8-carbamoyl-12-acetoxyheptadecanoate is replaced by an equimolar amount of ethyl 8-carbamoyl-12-hydroxy-12-methylheptadecanoate.

後処理

customThe synthesis of this compound

出典と根拠

ORDレコード: ord-d7751f82a5c3417e9b01675dc894f676
出典データセット: uspto-grants-1977_10
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US04055597

反応ノート

読み込み中…