化工社化工社 化学情報印刷レポート · 研究参考用
Sodium Hydroxide → 4-Methylhexylmethylmalonic acid
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Sodium Hydroxide | HCID 14798 | — |
| 反応物 | Diethyl 4-methylhexylmethylmalonate | HCID 54113602 | — |
| 溶媒 | Methanol | HCID 887 | — |
| 溶媒 | Water | HCID 962 | — |
| 生成物 | 4-Methylhexylmethylmalonic acid | HCID 54000156 | — |
反応手順
First, 8.18 g (0.22 mol) of sodium hydroxide was dissolved in a mixture solution of 28 ml of water and 14 ml of methanol, thus forming a solution. Next, g of the crude product (II), not refined, was added to the resultant solution and reacted with the solution at 20° C. for three to five hours, thereby obtaining 18.4 g of 4-methylhexylmethylmalonic acid (III). This reaction is represented as follows: ##STR4##
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05063058 |
| 出典データセット | uspto-grants-1991_11 |
| ORD ID | ord-940c9a4c925c424b8d6bdebca07d15d3 |
| 出典メモ | uspto-grants-1991_11 |