関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Methylmalonic Acid | HCID 487 | — |
| 反応物 | Dimethylamine | HCID 674 | — |
| 反応物 | Formaldehyde | HCID 712 | — |
| 溶媒 | Water | HCID 962 | — |
| 生成物 | 3-(Dimethylamino)-2-methylpropanoic acid | HCID 14073324 | — |
反応手順
In 1.0 ml of water was dissolved 1.5 g of methylmalonic acid, after which 1.26 g of a 50% aqueous dimethylamine solution and 0.96 ml of a 37% aqueous formaldehyde solution were added with stirring at 0° C., and the resulting mixture was stirred at 0° to 5° C. for 3 hours and then at 80° C. for 30 minutes.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US05064945 |
|---|
| 出典データセット | uspto-grants-1991_11 |
|---|
| ORD ID | ord-cc3d7a87fd854185b231c67ec2bf855a |
|---|
| 出典メモ | uspto-grants-1991_11 |
|---|
