化工社化工社 化学情報印刷レポート · 研究参考用
Toluene → Fenobucarb
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Toluene | HCID 1140 | — |
| 反応物 | Carbamic acid, N-methyl-, ethyl ester | HCID 7752 | — |
| 反応物 | 2-Butylphenol | HCID 18515 | — |
| 反応物 | Phosphorus pentachloride | HCID 24819 | — |
| 生成物 | Fenobucarb | HCID 19588 | — |
反応手順
To a solution of 2-sec butylphenol (1.5 g, 0.01 mole) and ethyl N-methylcarbamate (1.03 g, 0.01 mole), along with phosphorus pentachloride (1.05 g, 0.05 mole) in toluene (10 ml) was stirred at 28° C. and afterwards it was refluxed for 7 hours and worked up as usual to get the title compound.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05066819 |
| 出典データセット | uspto-grants-1991_11 |
| ORD ID | ord-f166edc01c3246aba7e7539f2255c21f |
| 出典メモ | uspto-grants-1991_11 |