反応式
[CH2:1]([C:5]1[CH:10]=[CH:9][CH:8]=[CH:7][C:6]=1[OH:11])[CH2:2][CH2:3]C.[CH3:12][NH:13][C:14](=O)[O:15]CC.P(Cl)(Cl)(Cl)(Cl)Cl.[C:25]1(C)C=CC=CC=1>>[CH3:12][NH:13][C:14](=[O:15])[O:11][C:6]1[CH:7]=[CH:8][CH:9]=[CH:10][C:5]=1[CH:1]([CH2:2][CH3:3])[CH3:25]参加物
5
実験手順
To a solution of 2-sec butylphenol (1.5 g, 0.01 mole) and ethyl N-methylcarbamate (1.03 g, 0.01 mole), along with phosphorus pentachloride (1.05 g, 0.05 mole) in toluene (10 ml) was stirred at 28° C. and afterwards it was refluxed for 7 hours and worked up as usual to get the title compound.
後処理
- temperatureafterwards it was refluxed for 7 hours
出典と根拠
- ORDレコード
- ord-f166edc01c3246aba7e7539f2255c21f
- 出典データセット
- uspto-grants-1991_11
- 特許番号
- US05066819
関連ノート
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