関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Water | HCID 962 | — |
| 反応物 | 3,7-Dimethyl-1-octanol | HCID 7792 | — |
| 反応物 | Phosphorus tribromide | HCID 24614 | — |
| 溶媒 | Hexane | HCID 8058 | — |
| 生成物 | 1-Bromo-3,7-dimethyloctane | HCID 137914 | — |
反応手順
To neat 3,7-dimethyloctanol (5 ml) was added phosphorus tribromide (1.01 ml). The mixture was stirred for 4 hours at 60° C. The reaction mixture was added to a mixture of water and n-hexane. The organic layer was separated and dried over magnesium sulfate. The magnesium sulfate was filtered off, and the filtrate was evaporated under reduced pressure to give 3,7-dimethyloctyl bromide (4.40 g).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | USH0001638 |
|---|
| 出典データセット | uspto-grants-1997_03 |
|---|
| ORD ID | ord-3494bf0f116242de84cf8586d6e3cba3 |
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| 出典メモ | uspto-grants-1997_03 |
|---|
