5-Acetyl-2,4-dimethyloxazole → 1-(4-Bromo-3-furyl)-1-(2,4-dimethyl-5-oxazolyl)ethanol

反応式

[C:1]([C:4]1[O:8][C:7]([CH3:9])=[N:6][C:5]=1[CH3:10])(=[O:3])[CH3:2].[Br:11][C:12]1[C:13]([Li])=[CH:14][O:15][CH:16]=1>>[Br:11][C:12]1[C:13]([C:1]([C:4]2[O:8][C:7]([CH3:9])=[N:6][C:5]=2[CH3:10])([OH:3])[CH3:2])=[CH:14][O:15][CH:16]=1

参加物

反応物 2

HCID 3184185-Acetyl-2,4-dimethyloxazole

HCID 178418340HCID 178418340、化合物

生成物 1

HCID 199708911-(4-Bromo-3-furyl)-1-(2,4-dimethyl-5-oxazolyl)ethanol

実験手順

Following the general method of Example 1a but using 5-acetyl-2,4-dimethyloxazole and 4-bromo-3-lithiofuran (Liebigs Ann. Chem., 1986, 625-637), the title compound was prepared.

出典と根拠

ORDレコード: ord-6281253b300842e39b4b08f721ddb383
出典データセット: uspto-grants-1997_03
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US05607956

反応ノート

読み込み中…