Hydrochloric Acid → HCID 86750549、化合物

HRID 976012ノート

反応式

HRID 976012 の反応式
C[O:2][C:3](=[O:16])[C@@H:4]([NH2:15])[CH2:5]/[CH:6]=[CH:7]/[CH2:8][C@H:9]([NH2:14])[C:10]([O:12]C)=[O:11].[ClH:17]>>[ClH:17].[ClH:17].[NH2:15][C@@H:4]([CH2:5]/[CH:6]=[CH:7]/[CH2:8][C@H:9]([NH2:14])[C:10]([OH:12])=[O:11])[C:3]([OH:16])=[O:2]

参加物

3

反応物 2

HCID 313Hydrochloric AcidHCID 71474603(S,S)-2,7-Diamino-(E)-oct-4-ene-1,8-dioic acid dimethyl ester

生成物 1

HCID 86750549HCID 86750549、化合物

実験手順

(S,S)-2,7-Diamino-(E)-oct-4-ene-1,8-dioic acid dimethyl ester (1.65 g, 7.17 mmol) was heated under reflux with 6H HCl (10 ml, 60 mmol) for 2 hours. The solvent was then evaporated, the residue was dissolved in water (10 ml) and ethanol was added (100 ml). The white crystals were filtered off and dried in vacuum at 40° C.

後処理

  1. customThe solvent was then evaporated
  2. dissolutionthe residue was dissolved in water (10 ml)
  3. additionethanol was added (100 ml)
  4. filtrationThe white crystals were filtered off
  5. customdried in vacuum at 40° C.

出典と根拠

ORDレコード
ord-e3de0dc4f3034c94952d772f35754d99
出典データセット
uspto-grants-1997_03
特許番号
US05610141

反応ノート

読み込み中…