化工社化工社 化学情報印刷レポート · 研究参考用
Methanol → 3-Methoxy-3-oxo-2-phenylpropanoic acid
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Methanol | HCID 887 | — |
| 反応物 | Boron trifluoride etherate | HCID 8000 | — |
| 反応物 | Phenylmalonic acid | HCID 75791 | — |
| 生成物 | 3-Methoxy-3-oxo-2-phenylpropanoic acid | HCID 2817775 | — |
反応手順
A mixture of phenylmalonic acid (3.6 g, 0.02 mol), boron trifluoride etherate (2.4 mL, 0.02 mol) and 0.8 mL of anhydrous methanol (0.02 mol) was refluxed and stirred for 24 hours. After cooling to room temperature, the reaction mixture was filtered and 20 mL of water was added.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05610188 |
| 出典データセット | uspto-grants-1997_03 |
| ORD ID | ord-9ce6dd16fcca45f9ab3aea345993b2d6 |
| 出典メモ | uspto-grants-1997_03 |