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Trifluoroacetic acid → (Benzyloxy)(methyl)amine
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Trifluoroacetic acid | HCID 6422 | — |
| 反応物 | tert-butyl N-benzyloxy-N-methylcarbamate | HCID 14227181 | — |
| 反応物 | tert-butyl N-benzyloxy-N-(2-methylpropyl)carbamate | HCID 19967428 | — |
| 生成物 | (Benzyloxy)(methyl)amine | HCID 13417387 | — |
反応手順
Using the general method of Compound 54 Part C, tert-butyl N-benzyloxy-N-methylcarbamate (3.0 g, 13 mmol) was reacted with trifluoroacetic acid (10 mL, 130 mmol) to provide 1.58 g of N-benzyloxy-N-methylamine as a yellow oil.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05612377 |
| 出典データセット | uspto-grants-1997_03 |
| ORD ID | ord-dfca262cc7444a829f0c340430c1b57e |
| 出典メモ | uspto-grants-1997_03 |