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Decyl chloroformate → Phthalimide hydrochloride
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Decyl chloroformate | HCID 108727 | — |
| 反応物 | N-[2-[4-(6-fluoro1H-indazol-3-yl)-1-piperazinyl]ethyl]phthalimide | HCID 18467209 | — |
| 溶媒 | Diethyl Ether | HCID 3283 | — |
| 生成物 | Phthalimide hydrochloride | HCID 22266261 | — |
反応手順
A mixture of decanyl chloroformate (2.4 g, 11 mmol), and N-[2-[4-(6-fluoro-1H-indazol-3-yl)-1-piperazinyl]ethyl]phthalimide (3.9 g, 10 mmol) was warmed on the steam bath for 15 minutes. The reaction was allowed to cool to ambient temperature, and then ether was added to the residue. The resulting solid was filtered to afford N2-[4-(1 -decanoxy-6-fluoro-1H-indazol-3-yl)-1-piperazinyl]ethyl]phthalimide hydrochloride.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05612343 |
| 出典データセット | uspto-grants-1997_03 |
| ORD ID | ord-94eabb6893cd4ead8af84e723c17a62a |
| 出典メモ | uspto-grants-1997_03 |