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HRID 978222作成日:2026年10月26日

3-Methyl-1,5-pentanediol → 3-Methyl-1,5-pentanediol

https://huagongshe.com/reaction/978222

反応式

関与物質

役割名称HCID仕込み量
反応物3-Methyl-1,5-pentanediolHCID 20524—
反応物beta-Methyl-delta-valerolactoneHCID 79142—
生成物3-Methyl-1,5-pentanediolHCID 20524—
生成物beta-Methyl-delta-valerolactoneHCID 79142—
生成物2-Hydroxy-4-methyltetrahydropyranHCID 11469063—

反応手順

According to the prior art methods, production of β-methyl-δ-valerolactone and 3-methylpentane-1,5-diol requires respective independent production facilities. On the contrary, the simultaneous production method can produce β-methyl-δ-valerolactone and 3-methylpentane-1,5-diol simultaneously from 2-hydroxy-4-methyltetrahydropyran with a common reactor and under relatively mild conditions. According to this simultaneous production method, β-methyl-δ-valerolactone and 3-methylpentane- 1,5-diol are produced generally in a β-methyl-δ-valerolactone/3-methylpentane-1,5-diol mole ratio of about 70/30 to 15/85. Said simultaneous production on method can give β-methyl-δ-valerolactone and 3-methylpentane- 1,5-diol each in a satisfactory yield and in a yield ratio therebetween selected depending on the demands therefor.

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US04663468
出典データセットuspto-grants-1987_05
ORD IDord-8e666ef7f2ad4eccb66242084493a35d
出典メモuspto-grants-1987_05