関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | 3-Methyl-1,5-pentanediol | HCID 20524 | — |
| 反応物 | beta-Methyl-delta-valerolactone | HCID 79142 | — |
| 生成物 | 3-Methyl-1,5-pentanediol | HCID 20524 | — |
| 生成物 | beta-Methyl-delta-valerolactone | HCID 79142 | — |
| 生成物 | 2-Hydroxy-4-methyltetrahydropyran | HCID 11469063 | — |
反応手順
According to the prior art methods, production of β-methyl-δ-valerolactone and 3-methylpentane-1,5-diol requires respective independent production facilities. On the contrary, the simultaneous production method can produce β-methyl-δ-valerolactone and 3-methylpentane-1,5-diol simultaneously from 2-hydroxy-4-methyltetrahydropyran with a common reactor and under relatively mild conditions. According to this simultaneous production method, β-methyl-δ-valerolactone and 3-methylpentane- 1,5-diol are produced generally in a β-methyl-δ-valerolactone/3-methylpentane-1,5-diol mole ratio of about 70/30 to 15/85. Said simultaneous production on method can give β-methyl-δ-valerolactone and 3-methylpentane- 1,5-diol each in a satisfactory yield and in a yield ratio therebetween selected depending on the demands therefor.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| 特許番号 | US04663468 |
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| 出典データセット | uspto-grants-1987_05 |
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| ORD ID | ord-8e666ef7f2ad4eccb66242084493a35d |
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| 出典メモ | uspto-grants-1987_05 |
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