ホームMCPワークベンチSkills
ホームワークベンチ通知マイページ
llms.txt · MCPガイドプライバシーポリシー · 利用規約 · サポートv1.8.0
  1. ホーム
  2. /反応

Hydrochloric Acid → 2,6-Dichloro-N-(((4-(2,2-dichloro-1,1-difluoroethoxy)phenyl)amino)carbonyl)-benzamide

HRID 978304
ノート
印刷プレビュー

反応式

HRID 978304 の反応式
[Cl:1][CH:2]([Cl:14])[C:3]([F:13])([F:12])[O:4][C:5]1[CH:10]=[CH:9][C:8]([NH2:11])=[CH:7][CH:6]=1.Cl.[Cl:16][C:17]1[CH:27]=[CH:26][CH:25]=[C:24]([Cl:28])[C:18]=1[C:19]([N:21]=[C:22]=[O:23])=[O:20]>C1(C)C(C)=CC=CC=1>[Cl:16][C:17]1[CH:27]=[CH:26][CH:25]=[C:24]([Cl:28])[C:18]=1[C:19]([NH:21][C:22]([NH:11][C:8]1[CH:7]=[CH:6][C:5]([O:4][C:3]([F:12])([F:13])[CH:2]([Cl:1])[Cl:14])=[CH:10][CH:9]=1)=[O:23])=[O:20]
参加物実験手順後処理出典と根拠反応ノート

参加物

5

反応物 3

HCID 313Hydrochloric AcidHCID 30172134-(2,2-Dichloro-1,1-difluoroethoxy)anilineHCID 129127392,6-Dichlorobenzoyl isocyanate

生成物 1

HCID 202023562,6-Dichloro-N-(((4-(2,2-dichloro-1,1-difluoroethoxy)phenyl)amino)carbonyl)-benzamide収率 463.9%

試薬・触媒・溶媒 1

HCID 7237O-Xylene溶媒

実験手順

In 200 milliliters of xylene, 11.5 grams (0.04 mole) of β,β-dichloro-α,α-difluoro-p-phenetidine.HCl and 3.6 grams (0.04 mole) of 2,6-dichlorobenzoyl isocyanate were refluxed with stirring for two hours. The xylene was thereafter removed by vacuum distillation. The residue which remained was mixed with 200 milliliters of hexane and a crystalline solid precipitated. This precipitated material was collected by suction filtration, washed with hexane and dried. The dried crude product was a light tan gummy solid melting at 160°-185° C. This crude product was purified by recrystallization from 60 milliliters of 83 percent aqueous acetic acid, leaving 85 grams of a white solid melting at 211°-213° C. (56 percent of theoretical). Nuclear magnetic resonance spectroscopy confirmed the structure as being ##STR13##

後処理

  1. customThe xylene was thereafter removed by vacuum distillation
  2. additionThe residue which remained was mixed with 200 milliliters of hexane
  3. customa crystalline solid precipitated
  4. filtrationThis precipitated material was collected by suction filtration
  5. washwashed with hexane
  6. customdried
  7. customThe dried crude product
  8. customThis crude product was purified by recrystallization from 60 milliliters of 83 percent aqueous acetic acid

出典と根拠

ORDレコード
ord-201f65ed6c634b5bb07ec2e26e37e2ea
出典データセット
uspto-grants-1987_05
DOI
10.6084/m9.figshare.5104873.v1
特許番号
USRE032418

反応ノート

読み込み中…

このページの内容参加物実験手順後処理出典と根拠反応ノート