関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Silane, ethenyltris(1-methylethoxy)- | HCID 87409 | — |
| 反応物 | Tris(tert-butoxy)silane | HCID 101075511 | — |
| 溶媒 | O-Xylene | HCID 7237 | — |
| 生成物 | 1-Tritertbutoxysilyl-2-triisopropoxysilylethylene | HCID 54208286 | — |
反応手順
Into a 45 cc Parr bomb was added 2.5 g (0.010 mol) tritertbutoxysilane, 4.7 g (0.020 mol) vinyltriisopropoxysilane, 1.0 g xylene and 2000 ppm Ru3CO12 (29 mg) as a catalyst. The reaction was heated to 225° C. for 3 hours in a fluidized sand bath. A single product, 1-tritertbutoxysilyl-2-triisopropoxysilylethylene was formed.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US04668812 |
|---|
| 出典データセット | uspto-grants-1987_05 |
|---|
| ORD ID | ord-ce0c828dc6334923bb02036296c792c4 |
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| 出典メモ | uspto-grants-1987_05 |
|---|
