関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Silane, ethenyltris(1-methylethoxy)- | HCID 87409 | — |
| 反応物 | Tris(propan-2-yloxy)silane | HCID 15722916 | — |
| 溶媒 | O-Xylene | HCID 7237 | — |
| 生成物 | 1,2-Bis(triisopropoxysilyl)ethylene | HCID 53828948 | — |
反応手順
Into a 45 cc Parr bomb was added 2.5 g (0.012 mol) triisopropoxysilane, 5.7 g (0.024 mol) vinyltriisopropoxysilane, 1.0 xylene and 200 ppm Ru3CO12 (20 mg). The reaction was heated for 4 hours at 225° C. in a fluidized sand bath. A single product, 1,2-bis(triisopropoxysilyl)ethylene was formed.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US04668812 |
|---|
| 出典データセット | uspto-grants-1987_05 |
|---|
| ORD ID | ord-1cfea45e05b949b0bff2e9a9f1f49b20 |
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| 出典メモ | uspto-grants-1987_05 |
|---|
