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Triethylamine → Chromium (II) bis(2-ethylhexanoate)
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Triethylamine | HCID 8471 | — |
| 反応物 | 2-Ethylhexanoic Acid | HCID 8697 | — |
| 反応物 | chromium(II) dichloride | HCID 10197677 | — |
| 溶媒 | Heptane | HCID 8900 | — |
| 生成物 | Chromium (II) bis(2-ethylhexanoate) | HCID 21922276 | — |
反応手順
Chromium (II) bis(2-ethylhexanoate) is prepared by the addition of an equimolar mixture of triethylamine and 2-ethylhexanoic acid in heptane to a suspension of 0.5 mole anhydrous chromium (II) chloride in heptane. A slow reaction results in the formation of a deep purple solution and the precipitation of triethylammonium hydrochloride. The product is isolated as a purple oil after removal of the precipitate by filtration and the volatiles under vacuum.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04668838 |
| 出典データセット | uspto-grants-1987_05 |
| ORD ID | ord-d2533a5280b044d7bc482e2666c224f8 |
| 出典メモ | uspto-grants-1987_05 |