化工社化工社 化学情報印刷レポート · 研究参考用
Glycine → N-Lauroylglycine
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Glycine | HCID 750 | — |
| 反応物 | Dodecanoyl chloride | HCID 8166 | — |
| 生成物 | Glycine | HCID 750 | — |
| 生成物 | Dodecanoyl chloride | HCID 8166 | — |
| 生成物 | N-Lauroylglycine | HCID 346152 | 94% |
反応手順
N-Lauroylglycine was prepared by reaction of lauroyl chloride with glycine according to the procedure described in Example I. From 109.4 g (0.500 mol) of lauroyl chloride and 37.6 g (0.500 mol) of glycine was obtained 120.5 g (94%) of N-lauroylglycine, mp 110°-118° C., lit mp 118°-119° C. [E. Jungerman, J. F. Gerecht, and I. J. Krems, J. Amer. Chem. Soc. 78, 172 (1956)].
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04634551 |
| 出典データセット | uspto-grants-1987_01 |
| ORD ID | ord-05ea4a946d69492d8f0906d75b52267d |
| 出典メモ | uspto-grants-1987_01 |