化工社化工社 化学情報印刷レポート · 研究参考用
Hydrogen Peroxide → Hydrogen Peroxide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Hydrogen Peroxide | HCID 784 | — |
| 反応物 | N-Lauroylglycine | HCID 346152 | — |
| 溶媒 | Methanesulfonic Acid | HCID 6395 | — |
| 生成物 | Hydrogen Peroxide | HCID 784 | — |
| 生成物 | N-Lauroylglycine | HCID 346152 | — |
| 生成物 | N-lauroylaminoperoxyacetic acid | HCID 54133591 | — |
反応手順
N-Lauroylaminoperoxyacetic acid was prepared by reaction of N-lauroylglycine with hydrogen peroxide in methanesulfonic acid according to the procedure described in Example II. From 50.0 g (0.195 mol) of N-lauroylglycine and 33.1 g (0.973 mol) of hydrogen peroxide in 100 mL methanesulfonic acid was obtained 38.0 g of N-lauroylaminoperoxyacetic acid having an AvO of 3.03% (theoretical yield=53.2 g having an AvO of 5.86%).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04634551 |
| 出典データセット | uspto-grants-1987_01 |
| ORD ID | ord-c28cded40e394c00b11c9f23f9f09404 |
| 出典メモ | uspto-grants-1987_01 |