Hydrogen Peroxide → HCID 12610196、化合物
反応式
[N:1]1[C:14]2[NH:13][C:12]3[C:7](=[CH:8][CH:9]=[CH:10][CH:11]=3)[S:6][C:5]=2[N:4]=[CH:3][CH:2]=1.[OH:15]O>C(O)(=O)C>[N:1]1[C:14]2[NH:13][C:12]3[C:7](=[CH:8][CH:9]=[CH:10][CH:11]=3)[S:6](=[O:15])[C:5]=2[N:4]=[CH:3][CH:2]=1参加物
4
実験手順
To 1,4-diaza-10H-phenothiazine (1 g, 5 mmoles) in acetic acid (15 ml) was added 50% hydrogen peroxide (1 ml). The mixture was stirred at 55° for 30 minutes. The mixture was evaporated to a small volume and the title compound crystallized out. The crystals were filtered, washed with acetic acid and air dried to yield 983 mg of the title compound, m.p. 261°-263°.
後処理
- customThe mixture was evaporated to a small volume
- customthe title compound crystallized out
- filtrationThe crystals were filtered
- washwashed with acetic acid and air
- customdried
出典と根拠
- ORDレコード
- ord-ccffd4cb476f4b6db33110fd996020c2
- 出典データセット
- uspto-grants-1987_01
- 特許番号
- US04634766
反応ノート
読み込み中…