化工社化工社 化学情報印刷レポート · 研究参考用
Hexachlorocyclotriphosphazene → Trichlorotriphenoxycyclotriphosphazene
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Hexachlorocyclotriphosphazene | HCID 220225 | — |
| 反応物 | Phenolate Sodium | HCID 4445035 | — |
| 生成物 | Trichlorotriphenoxycyclotriphosphazene | HCID 23418754 | — |
反応手順
Examples 8 to 12 below illustrate embodiments of the invention in which hexachlorocyclotriphosphazene (compound 1) is reacted first with sodium phenoxide to produce an intermediate (trischlorotrisphenoxycyclotriphosphazene), 19 which is then reacted without separation with sodium 4-nitrophenoxide to afford tris(4-nitrophenoxy)tris(phenoxy)cyclotriphosphazene 20. The nitro groups of 20 are reduced to afford the corresponding tris amino compound 21 which is then used according to Scheme I or Scheme II shown in FIG. 2 and FIG. 3, respectively.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04634759 |
| 出典データセット | uspto-grants-1987_01 |
| ORD ID | ord-26873eb24d11451683ca63ba9e279889 |
| 出典メモ | uspto-grants-1987_01 |