化工社化工社 化学情報印刷レポート · 研究参考用
Hydroxyacetonitrile → (Dodecylamino)acetonitrile
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Hydroxyacetonitrile | HCID 7857 | — |
| 反応物 | Dodecylamine | HCID 13583 | — |
| 溶媒 | Methanol | HCID 887 | — |
| 生成物 | (Dodecylamino)acetonitrile | HCID 222308 | — |
反応手順
In a flask of 500 ml provided with a magnetic stirrer, 4.56 gr of hydroxyacetonitrile (0.08 mol) were mixed at room temperature with 16.3 gr of dodecylamine (0.088 mol) in 250 ml of methanol. The mixture was allowed to stand for 16 hours at room temperature and methanol was evaporated. The obtained liquid was distilled under 10-2 mm Hg. The fraction distilling between 106° and 116° crystallizes after cooling.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04639468 |
| 出典データセット | uspto-grants-1987_01 |
| ORD ID | ord-062b5b872d41428695569fdb5abf608a |
| 出典メモ | uspto-grants-1987_01 |