化工社化工社 化学情報印刷レポート · 研究参考用
Boron, trifluoro(methanol)-, (T-4)- → Methyl 2-(3-methoxyphenyl)-5-oxo-1-phenylpyrrolidin-3-carboxylate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Boron, trifluoro(methanol)-, (T-4)- | HCID 11062313 | — |
| 反応物 | 2-(3-Methoxyphenyl)-5-oxo-1-phenylpyrrolidin-3-carboxylic acid | HCID 13361985 | — |
| 生成物 | Methyl 2-(3-methoxyphenyl)-5-oxo-1-phenylpyrrolidin-3-carboxylate | HCID 13362002 | — |
反応手順
A solution of 25.0 gm. of 2-(3-methoxyphenyl)-5-oxo-1-phenylpyrrolidin-3-carboxylic acid in 200 ml 10-15% boron fluoride-methanol was refluxed for 8 hours and upon following the workup for example 1C the product was obtained as an oil.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04639529 |
| 出典データセット | uspto-grants-1987_01 |
| ORD ID | ord-547bbf377ac84c26a22b0895622c04ce |
| 出典メモ | uspto-grants-1987_01 |