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p-Toluenesulfonic acid → Ditridecyl 2-bromosuccinate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | p-Toluenesulfonic acid | HCID 6101 | — |
| 反応物 | 1-Tridecanol | HCID 8207 | — |
| 反応物 | Bromosuccinic acid | HCID 73557 | — |
| 溶媒 | Toluene | HCID 1140 | — |
| 生成物 | Ditridecyl 2-bromosuccinate | HCID 20072149 | — |
反応手順
A mixture of 19.7 g. (0.1 mole) of bromosuccinic acid, 40.1 g. (0.2 mole) of tridecanol, 0.25 g. of p-toluenesulfonic acid and 200 ml. of toluene is refluxed for 7 hours, using a Dean-Stark trap. There is collected 3.6 ml. of H2O in the trap which is exactly the calculated amount for this reaction when completed.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04990652 |
| 出典データセット | uspto-grants-1991_02 |
| ORD ID | ord-d8480f33bd4548e6902f13e99b1fd1c8 |
| 出典メモ | uspto-grants-1991_02 |