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Isobutylbenzene → 4'-Isobutylacetophenone
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Isobutylbenzene | HCID 10870 | — |
| 反応物 | Acetyl fluoride | HCID 11204 | — |
| 溶媒 | Acetic Acid | HCID 176 | — |
| 生成物 | 4'-Isobutylacetophenone | HCID 93214 | — |
反応手順
Isobutylbenzene (IBB) (10.2 lb/hr) and a solution of HF containing 13 wt % HOAc and 12 wt % acetyl fluoride (AcF) (153 lb/hr) were fed into reactor 1 through line 4. The mixture was reacted at 60° C. for 1.5 hrs to produce the desired 4-isobutylacetophenone product.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04990681 |
| 出典データセット | uspto-grants-1991_02 |
| ORD ID | ord-d3b93062aae846dd972c13f70c9a7b8b |
| 出典メモ | uspto-grants-1991_02 |