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Water → N(4-hydroxy-3,5-di-tert-butylphenyl) stearamide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Water | HCID 962 | — |
| 反応物 | Dichloromethane | HCID 6344 | — |
| 反応物 | Hexane | HCID 8058 | — |
| 反応物 | Phenol, 2,6-bis(1,1-dimethylethyl)-4-nitroso- | HCID 70383 | — |
| 反応物 | HCID 178418361 | HCID 178418361 | — |
| 触媒 | Palladium | HCID 23938 | — |
| 生成物 | N(4-hydroxy-3,5-di-tert-butylphenyl) stearamide | HCID 19824186 | — |
反応手順
A 2 liter Parr bomb was charged with 210.5 g of 44.6% water wet (0.5 mole, pure, dry) 2,6-di-tert-butyl-4-nitrosophenol, 2.0 g of 5% Pd/C catalyst, 300 ml dichloromethane and 400 ml hexane. The nitrogen purged system was pressurized to 50 psi with hydrogen and the rate of hydrogen uptake noted. Hydrogenation was completed within one hour.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04990671 |
| 出典データセット | uspto-grants-1991_02 |
| ORD ID | ord-89e4a46da6b64ab080f7764d88a2ecde |
| 出典メモ | uspto-grants-1991_02 |