Carbon Dioxide → 1,7-Octadien-3-ol
反応式
C=CC=C.O.C(=O)=[O:7].[CH2:9](O)[CH:10]=[CH:11][CH2:12][CH2:13][CH2:14][CH:15]=[CH2:16]>CN(C)C=O>[CH2:9]=[CH:10][CH:11]([OH:7])[CH2:12][CH2:13][CH2:14][CH:15]=[CH2:16]参加物
6
実験手順
The thus deposited and separated palladium complex was placed again in the autoclave, to which 0.5 mol of 1,3-butadiene, 1 mol of water, 0.6 mol of carbon dioxide, and 63 ml of dimethyl formamide were fed afresh. Then, the reaction was conducted under the same conditions as mentioned above, with the consequence that 0.158 mol of 2,7-octadien-1-ol, and 0.016 mol of 1,7-octadien 3-ol were produced.
後処理
- customseparated palladium complex
出典と根拠
- ORDレコード
- ord-92996d6a6ae842e98deb3a833302f9b2
- 出典データセット
- uspto-grants-1991_02
- 特許番号
- US04990698
反応ノート
読み込み中…