化工社化工社 化学情報印刷レポート · 研究参考用
Pyridine → 4,4'-Dimethoxybenzil
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Pyridine | HCID 1049 | — |
| 反応物 | 4,4'-Dimethoxybenzoin | HCID 95415 | — |
| 触媒 | Copper Sulfate | HCID 24462 | — |
| 溶媒 | Water | HCID 962 | — |
| 生成物 | 4,4'-Dimethoxybenzil | HCID 71043 | — |
反応手順
A mixture of 27.5 g of copper sulfate (0.11 mol), 25 g of pyridine and 10 g of water was heated until the copper sulfate was completely dissolved. Then, 13.5 g of 2 (0.05 mol) was added, and the heating was continued for 2 hours.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04992351 |
| 出典データセット | uspto-grants-1991_02 |
| ORD ID | ord-2e28483408af42eba47815f29c103df2 |
| 出典メモ | uspto-grants-1991_02 |