化工社化工社 化学情報印刷レポート · 研究参考用
Isopropanol → Yttrium(iii) isopropoxide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Isopropanol | HCID 3776 | — |
| 反応物 | Yttrium | HCID 23993 | — |
| 触媒 | Zinc | HCID 23994 | — |
| 触媒 | Zincchloride | HCID 3007855 | — |
| 生成物 | Yttrium(iii) isopropoxide | HCID 11550724 | 70% |
反応手順
The same procedure described in Example 3 was utilized except that ZnCl2 was substituted for zinc metal but was not milled with the yttrium. The milled yttrium, without zinc metal or zinc chloride, was reacted with a solution of isopropanol (500 cc) and 3 grams of ZnCl2 over a 24 hour period. Work-up of the reaction mixture yielded 41.6 grams (a 70% yield) of yttrium isopropoxide.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04996300 |
| 出典データセット | uspto-grants-1991_02 |
| ORD ID | ord-dac3355981c3471781afc681e54aba5f |
| 出典メモ | uspto-grants-1991_02 |