化工社化工社 化学情報印刷レポート · 研究参考用
Triethoxysilane → 1,14-Bis(triethoxysilyl)tetradecane
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Triethoxysilane | HCID 13830 | — |
| 反応物 | Tetradeca-1,13-diene | HCID 30875 | — |
| 溶媒 | O-Xylene | HCID 7237 | — |
| 生成物 | 1,14-Bis(triethoxysilyl)tetradecane | HCID 22559811 | — |
反応手順
A mixture of 25 g of 1,13-tetradecadiene (Aldrich), 44.4 g of triethoxysilane (Shin-Etsu Silicone) and 0.1 mL of 3% xylene solution of a platinum complex of bis((vinyl dimethyl)disiloxane) was stirred at room temperature in a nitrogen atmosphere for 3 days. The resultant reaction mixture was purified by distillation, to obtain 1,14-bis(triethoxysilyl)tetradecane. Its structure was confirmed by NMR.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06864006B2 |
| 出典データセット | uspto-grants-2005_03 |
| ORD ID | ord-6b9d9ed70234478894a9c99f754256de |
| 出典メモ | uspto-grants-2005_03 |