化工社化工社 化学情報印刷レポート · 研究参考用
10,12-Pentacosadiynoic acid → Methyl 10,12-tricosadiynoate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 10,12-Pentacosadiynoic acid | HCID 538433 | — |
| 反応物 | 10,12-Tricosadiynoic Acid | HCID 538457 | — |
| 反応物 | Tda pda | HCID 131724780 | — |
| 溶媒 | Ethanol | HCID 702 | — |
| 生成物 | Methyl 10,12-tricosadiynoate | HCID 9968876 | — |
反応手順
Alcoholic Monomer Solution of TDA/PDA: 10,12-Tricosadiynoic acid (TDA, 6 gm GFS Chemicals) and 10,12-pentacosadiynoic acid (PDA, 0.9 gm GFS Chemicals) were dissolved in 60 ml ethanol (Fisher). The solution was slightly warmed and stirred. The solution (TDA/PDA) was filtered (Whatman No. 1) to remove residual polymer. Dye colorant could be added to the alcoholic monomer solution as an indicator. Standard organic solvent based dyes were added at 2 drops per ml.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06866863B2 |
| 出典データセット | uspto-grants-2005_03 |
| ORD ID | ord-af5005e6f13c4f7bb696258067e46415 |
| 出典メモ | uspto-grants-2005_03 |