化工社化工社 化学情報印刷レポート · 研究参考用
Sodium Carbonate → Tricalcium Phosphate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Sodium Carbonate | HCID 10340 | — |
| 反応物 | Calcium pyrophosphate (Ca2P2O7) | HCID 24632 | — |
| 反応物 | Aluminum Sulfate | HCID 24850 | — |
| 生成物 | Tricalcium Phosphate | HCID 24456 | — |
反応手順
In this method, the first reactant, 800 g of a 12% aqueous solution of aluminum sulfate was added to the reactor vessel, then the second reactant, an 18% aqueous solution of sodium carbonate, was metered into the vessel at a rate of 7 ml/minute until the pH reached 5.9. The reactants were mixed together for 20 minutes under agitation. Next, 54 grams of calcium pyrophosphate was added and the resulting slurry was mixed for 15 minutes with agitation and filtered and washed to a conductivity of about 2000 μmhos. The recovered wetcake was reslurried with 150 g of water and 200 g of a 1% FD&C Blue No. 1 aqueous solution to form a slurry of colored calcium phosphate colorant and this slurry was then mixed for approximately 1 hour.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06630019B2 |
| 出典データセット | uspto-grants-2003_10 |
| ORD ID | ord-a225f7a185e74e02bae100a1e0f1e151 |
| 出典メモ | uspto-grants-2003_10 |