Ethoxyquin → Retinol

反応式

[CH3:1][C:2]1[CH2:7][CH2:6][CH2:5][C:4]([CH3:9])([CH3:8])[C:3]=1/[CH:10]=[CH:11]/[C:12](/[CH3:24])=[CH:13]/[CH:14]=[CH:15]/[C:16](/[CH3:23])=[CH:17]/[CH2:18][O:19]C(C)=O.CCOC1C=C2C(C)=CC(C)(C)NC2=CC=1>>[CH3:1][C:2]1[CH2:7][CH2:6][CH2:5][C:4]([CH3:8])([CH3:9])[C:3]=1/[CH:10]=[CH:11]/[C:12](/[CH3:24])=[CH:13]/[CH:14]=[CH:15]/[C:16](/[CH3:23])=[CH:17]/[CH2:18][OH:19]

参加物

反応物 2

HCID 3293Ethoxyquin

HCID 638034Retinol, acetate

生成物 1

HCID 445354Retinol

実験手順

mixture of vitamin A acetate, 2.8 million IU/G unstab. (80% by weight) (BASF AG) and ethoxyquin (20% by weight) (Raluquin, Raschig AG) were run in at 60° C. via a heated pump unit.

後処理

customwere run in at 60° C. via a heated pump unit

出典と根拠

ORDレコード: ord-ef3ee44cf5574abaa8a8c7601bd53396
出典データセット: uspto-grants-2003_10
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US06632389B1

反応ノート

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