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2-Methyl-1-butanol → N-(phenylacetyl)valine 2-methylbutyl Ester
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 2-Methyl-1-butanol | HCID 8723 | — |
| 反応物 | (2S)-3-methyl-2-(2-phenylacetamido)butanoic acid | HCID 853958 | — |
| 生成物 | N-(phenylacetyl)valine 2-methylbutyl Ester | HCID 15481773 | — |
反応手順
Following General Procedure BC and using the N-(phenylacetyl)valine prepared in Step A above and 2-methylbutan-1-ol (Aldrich), the title compound was prepared as a diastereomeric mixture. The reaction was monitored by tlc on silica gel and purification was by filtration as described in the general procedure.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06632811B2 |
| 出典データセット | uspto-grants-2003_10 |
| ORD ID | ord-dd4e96332c8d4cb1a1d13b9d3530f049 |
| 出典メモ | uspto-grants-2003_10 |