化工社化工社 化学情報印刷レポート · 研究参考用
Cyclohexanecarboxaldehyde → (2-Cyclohexyl-imidazo[1,2-a]pyrazin-3-yl)-(6-isocyano-hexyl)-amine
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Cyclohexanecarboxaldehyde | HCID 16275 | — |
| 反応物 | Aminopyrazine | HCID 78747 | — |
| 反応物 | 1,6-Diisocyanohexane | HCID 3391105 | — |
| 溶媒 | Perchloric Acid | HCID 24247 | — |
| 生成物 | (2-Cyclohexyl-imidazo[1,2-a]pyrazin-3-yl)-(6-isocyano-hexyl)-amine | HCID 9883789 | — |
反応手順
Compound (3) was prepared in accordance with general instructions 1 from 1.0 ml aminopyrazine solution (0.1 M, MC), 0.575 ml 1,6-diisocyanohexane solution (0.2 M, MC), 0.500 ml cyclohexanecarbaldehyde solution (0.3 M, MC), and 10 μl perchloric acid (w=20%).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06638933B2 |
| 出典データセット | uspto-grants-2003_10 |
| ORD ID | ord-39fcd23a72df4c698000feee9e7929d3 |
| 出典メモ | uspto-grants-2003_10 |