化工社化工社 化学情報印刷レポート · 研究参考用
Tert-Butyl isocyanide → (2-Anthracen-9-yl-imidazo[1,2-a]pyrazin-3-yl)-tert-butyl-amine
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Tert-Butyl isocyanide | HCID 23577 | — |
| 反応物 | 9-Anthracenecarboxaldehyde | HCID 69504 | — |
| 反応物 | Aminopyrazine | HCID 78747 | — |
| 溶媒 | Perchloric Acid | HCID 24247 | — |
| 生成物 | (2-Anthracen-9-yl-imidazo[1,2-a]pyrazin-3-yl)-tert-butyl-amine | HCID 17937207 | — |
反応手順
Compound (30) was prepared in accordance with general instructions 1 from 1.0 ml 2-aminopyrazine solution (0.1 M, MC), 0.575 ml tert-butyl isocyanide solution (0.2 M, MC), 0.500 ml anthracene-9-carbaldehyde solution (0.3 M, MC), and 10 μl perchloric acid (w=20%). Calculated mass 366.5; found mass 367.3 (ESI-MS)
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06638933B2 |
| 出典データセット | uspto-grants-2003_10 |
| ORD ID | ord-37a8b151357044feb540d0a6fe07f897 |
| 出典メモ | uspto-grants-2003_10 |